Advanced Instrumentation Techniques PDF Notes |
B.Pharmacy 8th Semester Noteskarts
Syllabus
Unit: 1
Nuclear Magnetic Resonance spectroscopy
Principles of H-NMR and C-NMR, chemical shift, factors affecting chemical shift, coupling constant, Spin – spin coupling, relaxation, instrumentation and applications.
Mass Spectrometry-
Principles, Fragmentation, Ionization techniques- Electron impact, chemical ionization, MALDI, FAB, Analyzers -Time of flight and Quadrupole, instrumentation, applications.
Unit: 2
Thermal Methods of Analysis:
- Principles, instrumentation and applications of Thermogravimetric Analysis (TGA), Differential Thermal Analysis (DTA), Differential Scanning Calorimetry (DSC)
X-Ray Diffraction Methods:
- Origin of X-rays, basic aspects of crystals, X-ray Crystallography, rotating crystal technique, single crystal diffraction, powder diffraction, structural elucidation and applications.
Unit: 3
- Calibration and validation- as per ICH and USFDA guidelines.
- Calibration of following Instruments: Electronic balance, UV-Visible spectrophotometer, IR spectrophotometer, Fluorimeter, Flame Photometer, HPLC and GC.
Unit: 4
- Radio immune assay: Importance, various components, Principle, different methods, Limitation and Applications of Radio immunoassay.
- Extraction techniques: General principle and procedure involved in the solid phase extraction
and liquid-liquid extraction.